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How Temperature Affects Viscosity

  How Temperature Affects Viscosity: Viscosity can be defined as the internal friction that occurs as a material flow, relative to itself....

2017年12月26日星期二

Capillary viscometer instructions

Description of glass capillary viscometer

Glass capillary viscometer to determine the liquid viscosity and polymer molecular weight of important instruments, the measurement range up to tens of thousands of centistokes (mm2 / S). Advantages are ease of use and accuracy compared to other types of viscometers. So widely used in petroleum industry, chemical industry, and other industrial and scientific research.

The Ubbelohde capillary viscometer produced by our factory conforms to the technical requirements stipulated by relevant national standards and ministry standards. In order to expand international exchanges, but also according to the specifications of IOS-3105 international standards for production, welcome to order.

Working glass capillary viscometer instructions for use 
Capillary viscometer by structure, shape can be divided into Ukrainian, Fen's, Ping's, counter-current four. The viscosity of the sample they measured was kinematic viscosity. Has been widely used in petroleum, chemical, light industry, mechanical and electrical, defense, transportation, coal, metallurgy, medicine, food, papermaking, textile, research, institutions of higher learning and other units. Correct use of capillary viscometer is important to ensure accurate product quality and scientific data.

(A) washing and drying

Before using the viscometer must be washed, the general first with solvent residue dissolved in the viscometer repeated washing, and then alcohol or gasoline wash, and then fuming sulfuric acid or potassium dichromate wash 2-3 hours immersion, Finally rinse with tap water, distilled water and rinse, into the oven, heating to 150oC or so, or in the natural temperature upside down for days, so far.

(B) loading: (except Uzbek directly into the thick tube from outside)

Use a rubber ball with a small mouth (earbuds) or syringe to attach the small glass tube to the thick tube, hold the viscometer in the left hand, and block the thick tube mouth with your index finger. Turn the viscometer upside down and place the long glass tube with capillary Into the sample, pull the syringe, the sample is drawn to the second coil (so that the liquid level and the coil tangent), and then erected. After the countercurrent is installed, clamp the latex tube with the clamp and wrap it on the pipe that sucks the sample.

(C) thermostat and transfer vertical

The sample is placed on a viscometer thermostat shelf (clip), the capillary left, right, before and after the vertical transfer, measured at a constant temperature of 10 minutes, began to measure, note the first to the second coil Between the outflow time, the general election line three times (removed not normal) take the average.

(D) available capillary diameter, sample viscosity range, refer to the following table: (selected viscometer sample outflow time of not less than 200 seconds)


Kent Yuan (Mr.)
Hangzhou Zhongwang Technology Co., LTD.
Skype: kenyuan9023   Wechat/WhatsApp:+86 15068109723lei@zonwon.com  www.zonwontech.com
    

2017年12月20日星期三

Ubbelohde viscometer diameter and applicable solvent list


Capillary diameter mm: 0.37; Applicable solvents: Dioxane
Capillary diameter mm: 0.38; Applicable solvent: chloroform
Capillary diameter mm: 0.39; Applicable solvents: acetone
Capillary diameter mm: 0.41; Applicable solvent: ethyl acetate
Capillary diameter mm: 0.46; Applicable solvents: Ding Ding acetate, acetone (1: 1
Capillary diameter mm: 0.47; Applicable solvent: tetrahydrofuran
Capillary diameter mm: 0.48; Applicable solvents: n-heptane
Capillary diameter mm: 0.49; Applicable solvents: dichloroethane, toluene
Capillary diameter mm: 0.54; Applicable solvents: chlorobenzene, benzene, methanol, p-xylene, n-octane
Capillary diameter mm: 0.55; Applicable solvents: butyl acetate;
Capillary diameter mm: 0.57; Applicable solvents: dimethylformamide, water;
Capillary diameter mm: 0.59; Applicable solvents: dimethylacetamide;
Capillary diameter mm: 0.61; Applicable solvents: cyclohexane, dioxane
Capillary diameter mm: 0.64; Applicable solvents: ethanol;
Capillary diameter mm: 0.66; Applicable solvents: nitrobenzene
Capillary diameter mm: 0.705; Applicable solvents: cyclohexanone
Capillary diameter mm: 0.78; Applicable solvents: o-chlorophenol, n-butanol
Capillary diameter mm: 0.80; Applicable solvents: phenol, tetrachloroethane 1: 1;
Capillary diameter mm: 1.07; Applicable solvent: m-cresol

2017年12月5日星期二

Hangzhou Zhongwang Technology CO.,LTD Demonstrated New Products On Shanghai International Textile Industry Exhibition

Hangzhou Zhongwang Technology CO.,LTD Demonstrated New Products On Shanghai International Textile Industry Exhibition

Venue: Shanghai New International Expo Center
Hall: E3
Booth No. :  ,B21
Date: 2017.11.27 – 30
Address: 2345 Long Yang Road, Pudong, Shanghai, PR China
Main product: Viscometer, polymer dissolving machine,Pipette, Digestion reactor, Muffle furnace, Capillary tube washing machine.
On November 27, the 4-day "18th Shanghai International Textile Industry Exhibition" opens at Shanghai New International Expo Center (Pudong). Hangzhou Zhongwang Technology Co., Ltd. was invited to participate in the fair. We bring together with the newly developed IVS400, IVS800, and other new sample pre-processing devices.

The intelligent viscosity measurement system IVS400 adopts the unique design of pressing block mode to replace the traditional rubber cap connection,it also equipped with an adaptive infrared detection system of imported stainless steel optical fiber. Each test unit can operate independently to complete the whole process of viscosity measurement . Online cleaning module can be extended as well to reducing the operating intensity of the operator. Automatic Viscosity Measurement System IVS800 series are the domestic realization of automatic measurement, automatic calculation, automatic injection, automatic cleaning, automatic drainage.
Mr.Zhu, the chairman of company said Zhongwang Technology will promote intelligent manufacturing in the textile industry, speed up the realization of technological innovation and promote the full integration of automation and informationization in the field of chemical fiber, and strive for China's precision manufacturing and industrial control . Zhongwang always hold to the principle of "continuously creating excellent instruments and making experiments simpler" ,so as to provide customers with more comprehensive and efficient products and services.

Kent Yuan (Mr.)
Hangzhou Zhongwang Technology Co., LTD.
Skype: kenyuan9023   Wechat/WhatsApp:+86 15068109723lei@zonwon.com  www.zonwontech.com
    

2017年11月22日星期三

Using Ubbelohde viscometer to measure the molecular weight of polyacrylamide

Test Method: Use 85g / L sodium nitrate solution will be configured as a dilute solution sample, with Ubbelohde viscometer to determine the ultimate viscosity, according to empirical formula to calculate the molecular weight of the sample.

Reagent solution: 85g / L sodium nitrate solution
Equipment: Ubbelohde viscometer (capillary diameter 0.55mm)
Constant temperature water bath (can control 30 ℃ ± 0.1 ℃)
Stopwatch (division 0.1s)
Acid filtration funnel
The company is located in:
Experimental steps:
1. Determination of sodium nitrate solution outflow time
The clean, dry Ubbelohde viscometer vertically placed 30 ℃ ± 0.1 ℃ constant temperature water bath so that the U-viscometer D ball all submerged under the water.
Will be filtered through acid filtration funnel sodium nitrate solution was added to the Ubbelohde viscometer filling line between G, so far, constant temperature 10min-15min.
M tube set a hose, with the clip, use the ear ball to the sodium nitrate solution into the D ball half, remove the ear wash ball, open the M tube.
Measure the time it takes for the sodium nitrate solution to flow through the timed markers E, F with a stop watch. Repeated determination of three times, the error does not exceed 0.2s, whichever is the average t0.
2. Preparation of sample solution
Weigh 0.03 g of solid sample or equivalent amount of colloidal sample from a known 50 mL dry beaker to the nearest 0.2 mg and dissolve with sodium nitrate solution. All transferred to 100mL volumetric flask, diluted with sodium nitrate solution to the mark, shake.
3. Determine the outflow time of the sample solution
The outflow time t1 of the sample solution is determined by the first step method
4. Calculate the result according to the formula


Kent Yuan (Mr.)
Hangzhou Zhongwang Technology Co., LTD.
Skype: kenyuan9023   Wechat/WhatsApp:+86 15068109723lei@zonwon.com  www.zonwontech.com
    

2017年11月14日星期二

Using Ubbelohde viscometer one-point method to determine the intrinsic viscosity


Material: a triangular flask
Two 10ml pipettes
Ubbelohde viscometer (capillary 0.5mm)
A water bath (temperature control accuracy of ± 0.1 ℃)
A stopwatch
Rubber hose two sections
A syringe
Wash the ear ball one
The company is located in:
step:
1, the system solution: Take a certain amount of polymer, add 10mm solvent, make it completely dissolved, if necessary, heated.
2, constant temperature: installed device, stable temperature up and down changes 0.1 ℃.
3, plus the solution balance 5min: up and down into the capillary tube three times.
4, determination: measured three sets of data, so that the deviation but 0.2s.
5, Determination of solvent flow time.


data processing:
ηr = t / t0 (t is the solution flow time, t0 solvent time)
ηsp = ηr-1
[η] = [2 (ηsp-ηr)] / C (C is the concentration unit g / ml)
[η] = (ηSP / C) c = 0 = (ln ηr / C) c = 0 [η] = KMα
Remove the pipette has been pre-heated solution 10ml, into the viscometer, the same method, the installation of viscometer, the determination of the solution outflow time t. Then followed by adding 2.00,3.00,5.00,10.00 ml of distilled water.


Kent Yuan (Mr.)
Hangzhou Zhongwang Technology Co., LTD.
Skype: kenyuan9023   Wechat/WhatsApp:+86 15068109723lei@zonwon.com  www.zonwontech.com
    

2017年11月8日星期三

Various viscosity measurement formula


Kinematic viscosity: V = K * (t-Δt)
Dynamic viscosity: η = K * (t - Δt) * ρ
Limit Viscosity --- ISO 1628/1 Schulz-Blaschke formula: [η] = I / (1 + K '· I · C)
Ultimate Viscosity --- Huggins Formula: [η] = [(1 + 4KHηsp) 1/2 -1] / 2KH · C
Ultimate Viscosity --- Kraemer Formula: [η] = [1 - (1 - 4β lnηr) 1/2] / 2 β · C
Solvent-Solomon-Ciuta equation: [η] = [2 (ηsp-lnηr)] 1/2 / C
Limiting viscosity number --- Malone Maron formula: [η] = (γlnηr + ηsp) / (1 + γ) · C
The ultimate viscosity --- Dong's formula [η] = (2lnηr + ηsp) / 3 · C.
Limit Viscosity --- Billmeyer formula: [η] = (3lnηr + ηsp) / 4 · C
Limiting viscosity - Martin Martin Log I = log [η] + K [η] · C.
Limit Viscosity --- Linear Extrapolation: Measure the viscosities and logarithm viscosities of more than three different concentrations of dilute polymer solutions for linear extrapolation to determine the limiting viscosity.
Relative viscosity: ηr = (t - Δt) / (t0 - Δt0)
Viscosity number: I = (ηr-1) / C
K value for polyvinyl chloride and polyvinyl alcohol according to the Fickentscher formula: K = 1000 {a - 1 + [1 + (2 / C + 2+ a) a] 1/2} / (150 + 300C)
Where: a = 1.5 logηr
The above limit viscosity number measurement, such as the input Mark -houwink formula K, α value can be calculated viscosity average molecular weight.
M = ([η] / K) 1 / α


Gods in his heaven, all's rights with the world.

Kent Yuan (Mr.)
Hangzhou Zhongwang Technology Co., LTD.
Skype: kenyuan9023   Wechat/WhatsApp:+86 15068109723lei@zonwon.com  www.zonwontech.com
    

2017年11月6日星期一

The 18th International Exhibition on Textile Industry Exhibition Invitation

We hereby sincerely invite you to visit our booth at The 18th International Exhibition on Textile Industry. 

Venue: Shanghai New International Expo Center
Hall: E3
Booth No. :  ,B21
Date: 2017.11.27 – 30
Address: 2345 Long Yang Road, Pudong, Shanghai, PR China
Main product: Viscometer, polymer dissolving machine,Pipette, Digestion reactor, Muffle furnace, Capillary tube washing machine.



Gods in his heaven, all's rights with the world.

Kent Yuan (Mr.)
Hangzhou Zhongwang Technology Co., LTD.
Skype: kenyuan9023   Wechat/WhatsApp:+86 15068109723lei@zonwon.com  www.zonwontech.com